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 Fakultät für Chemie und Mineralogie
Institut für Analytische Chemie


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“50 and More Essential NMR Experiments”

A Detailed Guide

WILEY-VCH  2013
ISBN-10: 3527334831 // ISBN-13: 978-3527334834,

Contents

Preface

Chapter 1 The Organic Set of NMR Spectra

1.1       The 1H NMR Experiment
1.2       APT-13C NMR
1.3       COSY
1.4       NOESY
1.5       HSQC
1.6       HMBC                 

Chapter 2 Advanced Organic NMR Spectroscopy

2.1       2D J-Resolved 1H NMR Spectroscopy
2.2       ROESY
2.3       TOCSY
2.4       HSQC-TOCSY
2.5       HOESY
2.6       INADEQUATE
2.7       ADEQUATE
2.8       J-HMBC
2.9       Gated Decoupling          

Chapter 3 Selective Methods

3.1       Water suppression by Presaturation
3.2       Solvent Suppression by 1D-NOESY
3.3       Water Suppression by Soggy Excitation Sculpting
3.4       Solvent Suppression using WET
3.5       SELTOCSY
3.6       SELNOESY
3.7       SELINCOR
3.8       SELINQUATE
3.9       Band Selective HMBC   

Chapter 4 Heteronuclear NMR

4.1       11B NMR Spectroscopy
4.2       15N NMR Spectroscopy
4.3       17O NMR Spectroscopy
4.4       19F NMR Spectroscopy
4.5       29Si NMR Spectroscopy
4.6       57Fe NMR Spectroscopy
4.7       195Pt NMR Spectroscopy     
  

Chapter 5 Experiments in Physical Organic Chemistry

5.1       Measurement of the Spin–Lattice Relaxation Time T1
5.2       Measurement of the Spin–Spin Relaxation Time T2
5.3       Dynamic 1H NMR Spectroscopy
5.4       Diffusion Measurement with DOSY
5.5       Residual Dipolar Couplings (RDC)

Chapter 6 Organic Chemistry Applications

6.1       ASIS
6.2       Chirality Determination
6.3       Advanced Mosher Method
6.4       Quantitative NMR and Relaxation Reagents
6.5       Determination of Association Constant K
6.6       STD NMR
6.7       A Kinetic Experiment

Chapter 7 An Excursion to the Solid State and to Structural Biology

7.1       The CP/MAS Experiment
7.2       High-Resolution Magic-Angle Spinning
7.3       HN-HSQC
7.4       HNCA 

Chapter 8 Maintenance and Calibration

8.1       Calibration of Pulse Duration in the Transmitter Channel
8.2       Calibration of the Pulse Duration in the Indirect Channe
8.3       Shaped Pulses
8.4       Adiabatic pulses
8.5       Temperature Calibration in NMR
8.6       Calibration of Pulsed Field Gradients

Appendix

  • Answers
  • Pulse Programs
  • Elementary Product Operator Formalism Rules
  • Chemical Shift and Spin-Coupling Data for Strychnine
  • Picture Credits
  • Index